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Vol. 16 (2024)

MXene@c-MWCNT Adhesive Silica Nanofiber Membranes Enhancing Electromagnetic Interference Shielding and Thermal Insulation Performance in Extreme Environments

https://doi.org/10.1007/s40820-024-01398-1
Ziyuan Han
Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou 450002, People’s Republic of China
Yutao Niu
School of Nano‑Tech and Nano‑Bionics, University of Science and Technology of China, Hefei 230026, People’s Republic of China
Xuetao Shi
Shaanxi Key Laboratory of Macromolecular Science and Technology, School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an 710072, People’s Republic of China
Duo Pan
Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou 450002, People’s Republic of China
Hu Liu
Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou 450002, People’s Republic of China
Hua Qiu
Shaanxi Key Laboratory of Macromolecular Science and Technology, School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an 710072, People’s Republic of China
Weihua Chen
Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou 450002, People’s Republic of China
Ben Bin Xu
Mechanical and Construction Engineering, Faculty of Engineering and Environment, Northumbria University, Newcastle Upon Tyne NE1 8, UK
Zeinhom M. El‑Bahy
Department of Chemistry, Faculty of Science, Al-Azhar University, Nasr City 11884, Cairo, Egypt
Hua Hou
Mechanical and Construction Engineering, Faculty of Engineering and Environment, Northumbria University, Newcastle Upon Tyne NE1 8, UK
Eman Ramadan Elsharkawy
Department of Chemistry, Faculty of Science, Northern Border University, Arar, Saudi Arabia
Mohammed A. Amin
Department of Chemistry, College of Science, Taif University, P.O. Box 11099, 21944 Taif, Saudi Arabia
Chuntai Liu
Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou 450002, People’s Republic of China
Zhanhu Guo
Mechanical and Construction Engineering, Faculty of Engineering and Environment, Northumbria University, Newcastle Upon Tyne NE1 8, UK

Corresponding Author: Hu Liu

liuhu@zzu.edu.cn

Nano-Micro Letters, Vol. 16 (2024), Article Number: 195

Abstract

A lightweight flexible thermally stable composite is fabricated by combining silica nanofiber membranes (SNM) with MXene@c-MWCNT hybrid film. The flexible SNM with outstanding thermal insulation are prepared from tetraethyl orthosilicate hydrolysis and condensation by electrospinning and high-temperature calcination; the MXene@c-MWCNTx:y films are prepared by vacuum filtration technology. In particular, the SNM and MXene@c-MWCNT6:4 as one unit layer (SMC1) are bonded together with 5 wt% polyvinyl alcohol (PVA) solution, which exhibits low thermal conductivity (0.066 W m−1 K−1) and good electromagnetic interference (EMI) shielding performance (average EMI SET, 37.8 dB). With the increase in functional unit layer, the overall thermal insulation performance of the whole composite film (SMCx) remains stable, and EMI shielding performance is greatly improved, especially for SMC3 with three unit layers, the average EMI SET is as high as 55.4 dB. In addition, the organic combination of rigid SNM and tough MXene@c-MWCNT6:4 makes SMCx exhibit good mechanical tensile strength. Importantly, SMCx exhibit stable EMI shielding and excellent thermal insulation even in extreme heat and cold environment. Therefore, this work provides a novel design idea and important reference value for EMI shielding and thermal insulation components used in extreme environmental protection equipment in the future.


Highlights:
1 The SiO2 nanofiber membranes and MXene@c-MWCNT6:4 as one unit layer (SMC1) were bonded together with 5 wt% PVA solution.
2 When the structural unit is increased to three layers, the resulting SMC3 has an average electromagnetic interference SET of 55.4 dB and a low thermal conductivity of 0.062 W m−1 K−1.
3 SMCx exhibit stable electromagnetic interference shielding and excellent thermal insulation even in extreme heat and cold environment.

Keywords

SiO2 nanofiber membranes MXene@c-MWCNT Composite film Thermal insulation Electromagnetic interference shielding
Han, Ziyuan, Yutao Niu, Xuetao Shi, Duo Pan, Hu Liu, Hua Qiu, Weihua Chen, Ben Bin Xu, Zeinhom M. El‑Bahy, Hua Hou, Eman Ramadan Elsharkawy, Mohammed A. Amin, Chuntai Liu, and Zhanhu Guo. 2024. “MXene@c-MWCNT Adhesive Silica Nanofiber Membranes Enhancing Electromagnetic Interference Shielding and Thermal Insulation Performance in Extreme Environments”. Nano-Micro Letters 16 (May):195. https://doi.org/10.1007/s40820-024-01398-1.
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