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Vol. 15 (2023)

Boosting Interfacial Polarization Through Heterointerface Engineering in MXene/Graphene Intercalated-Based Microspheres for Electromagnetic Wave Absorption

https://doi.org/10.1007/s40820-023-01123-4
Ge Wang
Institute for Composites Science Innovation (InCSI), School of Materials Science and Engineering, Zhejiang University, 38 Zheda Road, Hangzhou 310027, People’s Republic of China
Changfeng Li
Institute for Composites Science Innovation (InCSI), School of Materials Science and Engineering, Zhejiang University, 38 Zheda Road, Hangzhou 310027, People’s Republic of China
Diana Estevez
Institute for Composites Science Innovation (InCSI), School of Materials Science and Engineering, Zhejiang University, 38 Zheda Road, Hangzhou 310027, People’s Republic of China
Peng Xu
Institute for Composites Science Innovation (InCSI), School of Materials Science and Engineering, Zhejiang University, 38 Zheda Road, Hangzhou 310027, People’s Republic of China
Mengyue Peng
Institute for Composites Science Innovation (InCSI), School of Materials Science and Engineering, Zhejiang University, 38 Zheda Road, Hangzhou 310027, People’s Republic of China
Huijie Wei
Institute for Composites Science Innovation (InCSI), School of Materials Science and Engineering, Zhejiang University, 38 Zheda Road, Hangzhou 310027, People’s Republic of China
Faxiang Qin
Institute for Composites Science Innovation (InCSI), School of Materials Science and Engineering, Zhejiang University, 38 Zheda Road, Hangzhou 310027, People’s Republic of China

Corresponding Author: Faxiang Qin

faxiangqin@zju.edu.cn

Nano-Micro Letters, Vol. 15 (2023), Article Number: 152

Abstract

Multi-layer 2D material assemblies provide a great number of interfaces beneficial for electromagnetic wave absorption. However, avoiding agglomeration and achieving layer-by-layer ordered intercalation remain challenging. Here, 3D reduced graphene oxide (rGO)/MXene/TiO2/Fe2C lightweight porous microspheres with periodical intercalated structures and pronounced interfacial effects were constructed by spray-freeze-drying and microwave irradiation based on the Maxwell–Wagner effect. Such approach reinforced interfacial effects via defects introduction, porous skeleton, multi-layer assembly and multi-component system, leading to synergistic loss mechanisms. The abundant 2D/2D/0D/0D intercalated heterojunctions in the microspheres provide a high density of polarization charges while generating abundant polarization sites, resulting in boosted interfacial polarization, which is verified by CST Microwave Studio simulations. By precisely tuning the 2D nanosheets intercalation in the heterostructures, both the polarization loss and impedance matching improve significantly. At a low filler loading of 5 wt%, the polarization loss rate exceeds 70%, and a minimum reflection loss (RLmin) of −67.4 dB can be achieved. Moreover, radar cross-section simulations further confirm the attenuation ability of the optimized porous microspheres. These results not only provide novel insights into understanding and enhancing interfacial effects, but also constitute an attractive platform for implementing heterointerface engineering based on customized 2D hierarchical architectures.


Highlights:


1 rGO/MXene/TiO2/Fe2C heterointerface porous microspheres prepared via scalable method to boost polarization.
2 Customization of hierarchical structure by precisely tuning 2D rGO/MXene intercalation.
3 Optimal reflection loss of -67.4 dB and EAB = 5.47 GHz at low filler loading of 5 wt%. Simulations showed the benefits of 2D nanosheets intercalation on polarization loss.

Keywords

MXene Hierarchical microspheres Interfacial polarization Spray-freeze-drying Microwave absorption
Wang, Ge, Changfeng Li, Diana Estevez, Peng Xu, Mengyue Peng, Huijie Wei, and Faxiang Qin. 2023. “Boosting Interfacial Polarization Through Heterointerface Engineering in MXene/Graphene Intercalated-Based Microspheres for Electromagnetic Wave Absorption”. Nano-Micro Letters 15 (June):152. https://doi.org/10.1007/s40820-023-01123-4.
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